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HomeUS EPA Method 8270 (Appendix IX): GC Analysis of Semivolatiles on Equity®-5 (30 m x 0.25 mm I.D., 0.50 μm)
US EPA Method 8270 (Appendix IX): GC Analysis of Semivolatiles on Equity®-5 (30 m x 0.25 mm I.D., 0.50 μm)
Conditions
| column | Equity-5, 30 m x 0.25 mm I.D., 0.5 µm (28092-U) |
| oven | 40 °C (2 min), 50 °C/min to 100 °C, 10 °C/min to 200 °C, 30 °C/min to 325 °C (7.5 min) |
| carrier gas | helium, pressure programmed, 20 psi (0.0 min), ramp to 80 psi (0.0 min), ramp to 16.5 psi (3 min), ramp to 25 psi (hold for remainder of run) |
| sample | 50 ng on-column of a 62 Supplemental Appendix IX list consisting of semivolatile standards, 6 internal standards, and 8 surrogates |
| injection | 1 µL, splitless (0.61 min) |
| liner | 4 mm I.D., single taper |
| inj. temp. | 280 °C, splitless (0.61 min) |
| detector | MSD, Scan range 45-450 amu, 325C |
Description
| Categories | Analytical Chromatography, GC Applications, Semivolatiles |
| Featured Industry | Environmental |
| Legal Information | Equity is a registered trademark of Sigma-Aldrich Co. LLC |
| Other Notes | Complementary products: Syringes Vials Gas Purification and Gas Management Inlet Liners, Glass Wool, and Specialized Hand Tools Septa and Specialized Hand Tools Column Ferrules, Nuts, and Specialized Hand Tools |
| suitability | application for GC |
Analyte
- 1,2,4,5-Tetrachlorobenzene
- 1,2-Dichlorobenzene-d4
- 1,3,5-Trinitrobenzene
- 1,3-Dinitrobenzene
- 1,4-Dichlorobenzene-d4
- 1,4-Dinitrobenzene
- 1,4-Dioxane
- 1,4-Naphthoquinone
- 1-Methylnaphthalene
- 1-Naphthylamine
- 2,3,4,6-Tetrachlorophenol
- 2,3,5,6-Tetrachlorophenol
- 2,4,6-Tribromophenol
- 2,6-Dichlorophenol
- 2-Acetylaminofluorene
- 2-Chlorophenol-d4
- 2-Fluorobiphenyl
- 2-Fluorophenol
- 2-Naphthylamine
- 2-Picoline
- 3-Methylcholanthrene
- 3-Methylphenol
- 4-Aminobiphenyl
- 4-Dimethylaminoazobenzene
- 4-Nitroquinoline-1-oxide
- 5-Nitro-o-toluidine
- 7,12-Dimethylbenz[a]anthracene
- Acenaphthene-d10
- Acetophenone
- Aniline
- Benzyl alcohol
- Chlorobenzilate
- Chrysene-d12
- Dialate-1
- Dialate-2
- Dibenzo[a,j]acridine
- Dimethoate
- Dinoseb
- Diphenylamine
- Disulfoton
- Ethyl methanesulfonate
- Famphur
- Hexachloropropene-1
- Isodrin
- Isosafrole
- Isosafrole-2
- Kepone
- Methapyrilene
- Methyl methanesulfonate
- Methyl parathion
- Naphthalene-d8
- Nitrobenzene-d5
- N-Nitrosodibutylamine
- N-Nitrosodiethylamine
- N-Nitrosomerpholine
- N-Nitrosomethylethylamine
- N-Nitrosopiperidine
- N-Nitrosopyrrolidine
- o,o,o-Triethyl phosphorothioate
- o-Toluidine
- Parathion
- Pentachlorobenzene
- Pentachloroethane
- Pentachloronitrobenzene
- Perylene-d12
- Phenacetin
- Phenanthrene-d10
- Phenol-d6
- Phenylenediamine
- Phorate
- Pronamide
- p-Terphenyl-d14
- Pyridine
- Safrole
- Sulfotep
- Thionazin
- α,α-Dimethylphenethylamine
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