Merck
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文件

194484

Sigma-Aldrich

O -（2,3,4,5,6-五氟苄基）羟胺 盐酸盐

≥98%

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别名:
PFBHA·HCl
线性分子式:
C6F5CH2ONH2·HCl
CAS号:
57981-02-9
分子量:
249.57
Beilstein:
4031190
EC 号:
261-057-7
MDL编号:
MFCD00012953
PubChem化学物质编号:
24851655
NACRES:
NA.22

检测方案

≥98%

形式

solid

mp

227 °C (subl.) (lit.)

溶解性

water: soluble 50 mg/mL, clear to slightly hazy, colorless

SMILES字符串

Cl.NOCc1c(F)c(F)c(F)c(F)c1F

InChI

1S/C7H4F5NO.ClH/c8-3-2(1-14-13)4(9)6(11)7(12)5(3)10;/h1,13H2;1H

InChI key

HVMVKNXIMUCYJA-UHFFFAOYSA-N

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相关类别

应用

使用O-（2,3,4,5,6-五氟苄基）盐酸羟胺：
  • 制备含酮基甾体肟。
  • 作为衍生化试剂，用于测定血栓素B 2、前列腺素、苦杏仁甙及多种醛类、酮类、酸类。
它是一种通用试剂，用于通过GC、GC-MS和其他方法检测含羰基化合物 。

包装

无底玻璃瓶。内含物在插入的融合锥体内。

储存分类代码

11 - Combustible Solids

WGK

WGK 3

闪点(°F)

Not applicable

闪点(°C)

Not applicable

个人防护装备

Eyeshields, Gloves, type N95 (US)

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Vicente Ferreira et al.
Journal of chromatography. A, 1122(1-2), 255-265 (2006-05-20)
This work presents a thorough study of some aspects critical to the quantitative performance of methods for the determination of volatile aldehydes previously derivatized to pentafluorobenzyl hydroxylamine oximes. The conclusions of the study are further applied to the validation of
S W Liou et al.
Bulletin of environmental contamination and toxicology, 80(4), 324-328 (2008-03-18)
This work studied the feasibility of using a solid phase microextraction (SPME) fiber for sampling and analysis of gaseous formaldehyde as well as particulate-bound formaldehyde from burning Chinese incense. The SPME fiber with PDMS/DVB coating were partially coated with o-(2,3,4,5,6-pentafluorobenzyl)-hydroxylamine
Yun-Gon Kim et al.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 893-894, 177-181 (2012-03-31)
Nucleotide diphosphate (NDP) sugars are widely present in antibiotics and glycoconjugates, such as protein- and lipid-linked oligosaccharides, where they act as substrates for glycosyltransferase in eukaryotes and prokaryotes. Among NDP sugars, NDP-4-keto sugars are key intermediates in the synthesis of
Chunhui Deng et al.
Rapid communications in mass spectrometry : RCM, 19(5), 647-653 (2005-02-09)
In the current work, a simple, rapid, accurate and inexpensive method was developed for the determination of acetone in human blood. The proposed method is based on derivatization with O-(2,3,4,5,6-pentafluorobenzyl)hydroxylamine hydrochloride (PFBHA), followed by headspace liquid-phase microextraction (HS-LPME) and gas
Chunhui Deng et al.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 810(2), 269-275 (2004-09-24)
Analysis of breath acetone has been used as a diagnostic tool for diabetes. Due to its nature of volatility and activity, it is very difficult to accurately measure the concentration of acetone in human breath by gas chromatography-mass spectrometry (GC-MS).
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