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Supelco

SUPELCOWAX 10 Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.25 μm

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eCl@ss:
32119290

material

fused silica

Agency

OSHA 52,80
meets requirements for USP G16

parameter

35-280 °C temperature (isothermal or programmed)

Beta value

250

df

0.25 μm

technique(s)

gas chromatography (GC): suitable

L × I.D.

30 m × 0.25 mm

matrix active group

Bonded; poly(ethylene glycol) phase

application(s)

agriculture
chemicals and industrial polymers
cleaning products
cosmetics
flavors and fragrances
food and beverages
industrial hygiene
personal care
petroleum
pharmaceutical (small molecule)

column type

capillary polar

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General description

Application: This column is based on one of the most widely used polar phases, Carbowax 20M, and is a polar column suitable for analyses of solvents, fatty acid methyl esters (FAMEs), food, flavor and fragrance compounds, alcohols, and aromatics. Additionally, this column is a great choice when a polar general purpose column is required.
USP Code: This column meets USP G16 requirements.
Phase:
  • Bonded
  • Poly(ethylene glycol)
Temp. Limits:
  • ≤0.32 mm I.D.: 35 °C to 280 °C (isothermal or programmed)
  • ≥0.53 mm I.D., <2 μm: 35 °C to 280 °C (isothermal or programmed)
  • ≥0.53 mm I.D., ≥2 μm: 35 °C to 250 °C (isothermal or programmed)

Application

SUPELCOWAX 10 Capillary GC Column may be used for the analysis of milk fat in order to demonstrate its health benefits. It may also be used for high-resolution separation of polychlorinated biphenyls by comprehensive two-dimensional gas chromatography.

Other Notes

We offer a variety of chromatography accessories including analytical syringes

Legal Information

SUPELCOWAX is a trademark of Sigma-Aldrich Co. LLC

Storage Class Code

11 - Combustible Solids

WGK

WGK 3

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable


Certificates of Analysis (COA)

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  1. Which document(s) contains shelf-life or expiration date information for a given product?

    If available for a given product, the recommended re-test date or the expiration date can be found on the Certificate of Analysis.

  2. How do I get lot-specific information or a Certificate of Analysis?

    The lot specific COA document can be found by entering the lot number above under the "Documents" section.

  3. How do I use Product No. 47302 Polar Column Test Mix?

    Test the column using our test mix Product No. 47302 under the same conditions as in the Certificate of Analysis and compare the chromatograms.

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L W Getzin et al.
Journal - Association of Official Analytical Chemists, 72(2), 361-364 (1989-03-01)
A method for extraction, cleanup, and simultaneous gas chromatographic detection of carbofuran, metalaxyl, and simazine in soils has been developed. Pesticide residues were extracted from soil with acetone containing 10% 0.2M HCl-KCl buffer (pH 2.0), cleaned up with methylene chloride-carbonate
Yonghong Zhu et al.
Food chemistry, 109(4), 899-908 (2008-08-15)
A gas chromatography electron capture detector (GC-ECD) using the standard addition method was developed for the determination of acrylamide in heat-processed foods. The method entails extraction of acrylamide with water, filtration, defatting with n-hexane, derivatization with hydrobromic acid and saturated
J J Myher et al.
Journal of biochemical and biophysical methods, 15(2), 111-121 (1987-11-01)
The 5 alpha-stanol-3 beta-ol analogs of cholesterol, campesterol and beta-sitosterol along with many other sterol types were resolved using a Supelcowax 10 (Bonded Carbowax PEG 20M) fused silica capillary column (15 m x 0.25 mm). Unlike non-polar capillary columns, the
Andréa Figueiredo Procópio de Moura et al.
Archivos latinoamericanos de nutricion, 52(2), 207-211 (2002-08-20)
The objective of this study was to describe the fresh cooled pink-shrimp (Penaeus brasiliensis and Penaeus paulensis) lipid. The total lipid content was 1.13 +/- 0.09 g/100 g while fatty acid profile showed 32.9% saturated, 20.4% monounsaturated and 40.5% polyunsaturated.
Peter Korytár et al.
Journal of chromatography. A, 958(1-2), 203-218 (2002-07-24)
Comprehensive two-dimensional gas chromatography (GC x GC) with micro electron-capture detection (microECD) has been optimised for the separation of polychlorinated biphenyl congeners with emphasis on the separation of 12 toxic non- and mono-ortho chlorinated biphenyls (CBs), viz. CBs 77, 81

Protocols

This column is based on one of the most widely used polar phases, Carbowax 20M, and is a polar column suitable for analyses of solvents, fatty acid methyl esters (FAMEs), food, flavor and fragrance compounds, alcohols, and aromatics.

Separation of 2-Ethyl-3-methylpyrazine; 1-Methylpyrrole; 2,3-Dimethylpyrazine; 2,5-Dimethylpyrazine; 2-Ethylpyrazine, ≥98%, FG; 2,3-Diethylpyrazine; 2-Methylpyrazine; Carbon disulfide; Dimethyl disulfide; 2,6-Dimethylpyrazine

-(+)-Limonene, purum, ≥98.0% (sum of enantiomers, GC); Geranyl tiglate; α-Terpineol, natural, ≥96%, FCC, FG; Geranyl formate; α-Pinene

Chromatograms

suitable for GC, application for SPMEsuitable for GCsuitable for GCsuitable for GCShow More

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