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25467

Supelco

Carboxen®-1010 PLOT Capillary GC Column

L × I.D. 30 m × 0.53 mm, average thickness 30 μm

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Synonym(s):
Carboxen® 1010 PLOT Column, 30m x 0.53mm
EC Number:
eCl@ss:
32119290

material

fused silica

Agency

ASTM® D3612-96

description

PLOT = Porous Layer Open Tubular

manufacturer/tradename

Carboxen®

parameter

≤25-250 °C temperature (isothermal or programmed)

average thickness

30 μm

df

30 μm

technique(s)

gas chromatography (GC): suitable

L × I.D.

30 m × 0.53 mm

matrix active group

Carbon molecular sieve phase

application(s)

chemicals and industrial polymers
food and beverages

column type

capillary PLOT

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General description

Carboxen® Adsorbent is ideally used for solid-phase microextraction (SPME) and does highly efficient extraction of small polar molecules from aqueous solution. Porous-layer open-tubular (PLOT) columns are a powerful tool employed in gas chromatography during analysis of fixed gases, light hydrocarbons and volatile solvents. They are mostly preferred over traditional packed columns.
Application: This column is ideal for the separation of all major components in permanent gas (helium, hydrogen, oxygen, nitrogen, carbon monoxide, methane, and carbon dioxide) and light hydrocarbons (C2-C3) in the same analysis. It is the only column commercially available that is able to separate all major components in permanent gas. This column can also separate oxygen from nitrogen at subambient temperatures.
USP Code: None
Phase:
  • Carbon molecular sieve
Temp. Limits:
  • Subambient to 250 °C (isothermal or programmed)

Other Notes

We offer a variety of chromatography accessories including analytical syringes

Legal Information

ASTM is a registered trademark of American Society for Testing and Materials
Carboxen is a registered trademark of Merck KGaA, Darmstadt, Germany

Certificates of Analysis (COA)

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  1. Which document(s) contains shelf-life or expiration date information for a given product?

    If available for a given product, the recommended re-test date or the expiration date can be found on the Certificate of Analysis.

  2. How do I get lot-specific information or a Certificate of Analysis?

    The lot specific COA document can be found by entering the lot number above under the "Documents" section.

  3. What is the film thickness of the Carboxen-1010 PLOT Capillary GC Column, Product 25467?

    The film thickness for this column is 30um.  The term "film" is somewhat of a misnomer because it is actually a layer of solid carboxen particles adhered to the fused silica tubing.

  4. What types of compounds would be suitable for analysis on the Carboxen-1010 PLOT Capillary GC Column, Product 25467?

    This column is designed for the analysis of permanent gases and light hydrocarbons up to a maximum of 3 carbon units.

  5. Is the Carboxen 1010 PLOT column, Product 25467, GC/MS compatible?

    Yes, the particles are very strongly adhered to the surface of the column and would be compatible with mass spec detection.

  6. Is this product a packed column?

    This is packing material only; it is not a column. Some endusers will purchase this bottle of packing and prepare their own packed columns.

  7. How can I purchase a column that is packed with this material?

    Most packed column are custom made and require that you obtain a quotation. Please contact our Customer & Sales Services group at phone number (800)-247-6628, fax number (800)-447-3044 or email CIBelle@sial.com for additional information.

  8. How do I find price and availability?

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  9. What is the Department of Transportation shipping information for this product?

    Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product. 

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Applications of Solid Phase Microextraction
Pawliszyn J.
Applications of Solid Phase Microextraction, 64-65 (1999)
Porous layer open-tubular capillary columns: preparations, applications and future directions.
Zhenghua Ji
Journal of Chromatography A, 842 (1), 115-142 (1999)
Frank Sporkert et al.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 772(1), 45-51 (2002-05-23)
A new and in part automated headspace solid-phase microextraction method for quantitative determination of the highly toxic rodenticide fluoroacetic acid (FAA) in serum and other biological samples has been developed. FAA and deuterated acetic acid (internal standard) were extracted from
Shih-Wei Tsai et al.
Journal of chromatography. A, 991(1), 1-11 (2003-04-22)
The solid-phase microextraction (SPME) device was used as a time-weighted average (TWA) sampler for ethylene oxide. Carboxen/polydimethylsiloxane (CAR/PDMS) fiber was used and hydrogen bromide (HBr) was loaded onto the fiber. The SPME fiber assembly was then inserted into PTFE tubing
Licia Scibetta et al.
Analytica chimica acta, 581(1), 53-62 (2007-03-28)
Methyl tert-butyl ether (MTBE), ethyl tert-butyl ether (ETBE) and tert-amyl methyl ether (TAME) are oxygenated compounds added to gasoline to enhance octane rating and to improve combustion. They may be found as pollutants of living and working environments. In this

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