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About This Item
UNSPSC Code:
41115712
NACRES:
NB.21
Quality Level
material
PE frit, polypropylene hardware
product line
Supelclean™
composition
bed wt., 1 g
packaging
pkg of 30 ea
technique(s)
solid phase extraction (SPE): suitable
surface area
475 m2/g
volume
6 mL
matrix
silica gel base material (irregularly shaped)
matrix active group
silica bonding
particle size
45 μm
pore size
0.8 cm3/g pore volume, 60 Å pore size
application(s)
food and beverages
separation technique
normal phase
General description
Supelclean™ LC-Si SPE tube is used to extract polar analytes from nonpolar samples.
Application
Supelclean™ LC-Si SPE Tube may be used for the solid-phase extraction of:
- Phospholipids in dairy products prior to their determination by high performance liquid chromatography-evaporative light scattering detector (HPLC-ELSD).
- Free and esterified sterols in Portuguese olive oils prior to their estimation by gas chromatography-mass spectrometry (GC-MS).
- Synthetic musks in cream prior to their quantification by GC combined with tandem mass spectrometry (MS/MS).
- Phospholipids in milk samples prior to their quantification by hydrophilic interaction liquid chromatography (HILIC) in conjunction with ELSD as well as ion trap-time-of-flight mass spectrometry (IT-TOF MS).
Legal Information
Supelclean is a trademark of Sigma-Aldrich Co. LLC
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Storage Class
11 - Combustible Solids
wgk
nwg
flash_point_f
Not applicable
flash_point_c
Not applicable
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Protocols
(soybean), ≥97%; L-α-Phosphatidylethanolamine from egg yolk, Type III, ≥97% (TLC), lyophilized powder; L-α-Phosphatidylcholine, from egg yolk, Type XVI-E, ≥99% (TLC), lyophilized powder; Sphingomyelin, from chicken egg yolk, ≥95%
Quantification of free and esterified sterols in Portuguese olive oils by solid-phase extraction and gas chromatography-mass spectrometry.
Cunha SS, et al.
Journal of Chromatography A, 1128(1-2), 220-227 (2006)
Analysis of 7 synthetic musks in cream by supported liquid extraction and solid phase extraction followed by GC-MS/MS.
Dong H, et al.
Talanta, 120(1-2), 248-254 (2014)
Determination of phospholipids in dairy products by SPE/HPLC/ELSD.
Avalli A and Contarini G
Journal of Chromatography A, 1071(1-2), 185-190 (2005)
Global Trade Item Number
| SKU | GTIN |
|---|---|
| 57051 | 04061833667934 |