coated tip
coated tip
coated tip
coated tip
Standard was diluted in 10 mL isopropanol, sample was directly applied to the plate by CAMAG ATS4 6 mm bandwise.
1.15161 HPTLC Silica gel 60 RP-18 F 254s MS-grade 20cm x 10 cm (1.151161.0001)
[A] methanol; [B] acetonitrile; (9:1, A:B)
6 cm
normal chamber without chamber saturation
0.150 μL
UV, 254 nm (Identification by coupling the TLC – MS Interface (CAMAG) with the Advion expression) (CMS mass spectrometer (+)-ESI mode. Eluent: Acetonitrile / Water 95:5 + 0.1% TFA.)