CN
TLC Analysis Of Paracetamol in Different Formulations on HPTLC Silica Gel 60 F254 MS-grade
Materials
accessory
Product No.
Description
Pricing
Hamilton® TLC syringes
1702, volume 25 μL, needle size 22s ga, needle L 51 mm (2 in.),coated tip
Hamilton® TLC syringes
1705, volume 50 μL, needle size 22 ga, needle L 51 mm (2 in.),coated tip
Hamilton® TLC syringes
1701, volume 10 μL, needle size 26s ga, needle type, fixed, needle L 51 mm (2 in.),coated tip
Hamilton® TLC syringes
1710, volume 100 μL, needle size 22 ga, needle L 51 mm (2 in.),coated tip
CONDITIONS
plate
1.00934 HPTLC Silica gel 60 F254 MS-grade 20 cm x10 cm (1.00934.0001)
eluent
[A] aceton; [B] toluene; (1:1, A:B) containing 0.1% Acetic acid
migration distance
5 cm
chamber
normal chamber without chamber saturation
detector
UV, 254 nm
Description
Analysis Note
Sample prep: Suppository: One suppository containing 125 mg Paracetamol was diluted in
125 ml ethanol at 36°C and applied directly.
Pain syrup: 0.2 ml Paracetamol pain syrup containing 4 % Paracetamol was diluted in 7.8 ml methanol and applied directly.
Pill: One pill containing 500 mg Paracetamol was diluted in 500 ml methanol, filtered through a 0.45 μm Millex®-LCR syringe filter and applied directly.