反应适用性
core: palladium
reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Heck Reaction
reaction type: Hiyama Coupling
reaction type: Negishi Coupling
reaction type: Sonogashira Coupling
reaction type: Stille Coupling
reaction type: Suzuki-Miyaura Coupling
reagent type: catalyst
reaction type: Cross Couplings
应用
Step-by-Step Guide for KitAlysis™ High-Throughput Copper C-N Cross-Coupling Reaction Screening Kit
Downloadable experimental excel sheet
Each kit contains 2 customizable screening sets that include the following components:
- 24 (6 x 4) pre-weighed ligands in glass vials loaded with stir bars, topped with cap mat
- Potassium phosphate: 4 pre-weighed vials with product labels and lids
- CuI (soluble source) in preweighed vial
- 4 degassed anhydrous solvents (dioxane, DMAc, toluene, and DMSO) in ampules
- 1 internal standard
- 2 KitAlysis 24-Well reaction block replacement films
- 8 stir bars for stock solutions
- Ampule cracker
Monitor reaction progress via TLC-MS by following this protocol
Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).
特点和优势
- Designed and tested by synthetic chemists.
- Easily run 24-microscale reaction in parallel.
- Suggested conditions: 10 μmol reactions with 1 μmol catalyst (10 mol%) 0.1 M concentration, and 3 equiv. base.
- Customizable and downloadable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.
法律信息
警示用语：
Danger
危险分类
Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Asp. Tox. 1 - Carc. 1B - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2 Inhalation
靶器官
Central nervous system
补充剂危害
储存分类代码
3 - Flammable liquids
WGK
WGK 3
闪点(°F)
39.2 °F
闪点(°C)
4 °C
分析证书(COA)
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示例
其它示例：
705578-5MG-PW
PL860-CGA/SHF-1EA
MMYOMAG-74K-13
1000309185
输入内容 1.000309185)
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